ASTM D3654

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1、Designation:D3654/D3654M 06(Reapproved 2019)Standard Test Methods forShear Adhesion of Pressure-Sensitive Tapes1This standard is issued under the xed designation D3654/D3654M;the number immediately following the designation indicates theyear of original adoption or,in the case of revision,the year o

2、f last revision.A number in parentheses indicates the year of lastreapproval.A superscript epsilon()indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the U.S.Department of Defense.1.Scope1.1 This test method covers procedures f

3、or determining theability of pressure-sensitive tapes and labels to remain adheredunder constant load applied parallel to the surface of the tapeand substrate.1.1.1 Procedure A measures the shear adhesion when ap-plied to a vertical standard steel panel.1.1.2 Procedure B measures the shear adhesion

4、when ap-plied to vertical panel covered with NIST SRM 1810Astandard berboard.1.1.3 Procedure C measures the shear adhesion when ap-pliedtoaverticalpanelcoveredwithaberboardasdenedbyComite Europeen de Normalisation(CEN).1.1.4 Procedure D measures shear adhesion when applied toa vertical panel covered

5、 with a berboard agreed upon by thebuyer and seller.1.1.5 Procedure E measures shear adhesion of lamentreinforced tape when applied to a horizontal standard steelpanel.1.1.6 Procedure F measures shear adhesion of a lamentreinforced tape when applied to a horizontal panel coveredwith NIST SRM 1810A s

6、tandard berboard.1.1.7 ProcedureGmeasurestheshearadhesionofalamentreinforced tape when applied to a horizontal panel coveredwith a standard berboard dened by CEN.1.1.8 Procedure H measures the shear adhesion the same asProcedure A except the test is conducted at an elevatedtemperature and after a 10

7、-min dwell time at the elevatedtemperature.1.2 These procedures provide a means of assessing theuniformity of the adhesive of a given type of pressure-sensitivetape,usually tapes used for packaging applications.Theassessment may be within a roll of tape,between rolls orproduction lots.1.2.1 Variatio

8、ns in the tape backing and adhesive affect theresponse;therefore,these procedures cannot be used to pin-point the specic cause(s)of nonuniformity.1.2.2 This test method is intended to replace AFERA 4012,CEN 1943,and PSTC(see 7.2).1.3 The values stated in either SI units or inch-pound unitsare to be

9、regarded separately as standard.The values stated ineach system are not be exact equivalents;therefore,eachsystem shall be used independently of the other.Combiningvalues from the two systems will result in non-conformancewith the standard.1.4 This standard does not purport to address all of thesafe

10、ty concerns,if any,associated with its use.It is theresponsibility of the user of this standard to establish appro-priate safety,health,and environmental practices and deter-mine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accor-dance wit

11、h internationally recognized principles on standard-ization established in the Decision on Principles for theDevelopment of International Standards,Guides and Recom-mendations issued by the World Trade Organization TechnicalBarriers to Trade(TBT)Committee.2.Referenced Documents2.1 ASTM Standards:2A6

12、66 Specication forAnnealed or Cold-WorkedAusteniticStainless Steel Sheet,Strip,Plate,and Flat BarD3715/D3715M Practice for QualityAssurance of Pressure-Sensitive TapesD4332 Practice for Conditioning Containers,Packages,orPackaging Components for TestingD5750/D5750M Guide for Width and Length of Pres

13、sure-Sensitive TapeE122 Practice for Calculating Sample Size to Estimate,WithSpecied Precision,the Average for a Characteristic of aLot or Process1This test method is under the jurisdiction of ASTM Committee D10 onPackaging and is the direct responsibility of Subcommittee D10.14 on Tape andLabels.Cu

14、rrent edition approved Aug.1,2019.Published August 2019.Originallyapproved in 1978.Last previous edition approved in 2011 as D3654/D3654M 06(2011).DOI:10.1520/D3654_D3654M-06R19.2For referenced ASTM standards,visit the ASTM website,www.astm.org,orcontact ASTM Customer Service at serviceastm.org.For

15、Annual Book of ASTMStandards volume information,refer to the standards Document Summary page onthe ASTM website.Copyright ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959.United StatesThis international standard was developed in accordance with internationally rec

16、ognized principles on standardization established in the Decision on Principles for theDevelopment of International Standards,Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade(TBT)Committee.1 2.2 AFERA Standard:AFERA 4012 Self-Adhesive TapesMeasurement of

17、StaticShear Adhesion32.3 CEN Standard:EN 1943 Self-Adhesive TapesMeasurement of StaticShear Adhesion42.4 PSTC Standard:PSTC-7 Holding Power of Pressure-Sensitive Tapes53.Summary of Test Method3.1 Procedure A,Shear Adhesion to Standard SteelPanelAstripoftapeisappliedtoastandardsteelpanelundercontroll

18、ed roll down.The panel is mounted vertically,astandard mass is attached to the free end of the tape and thetime to failure is determined.3.2 Procedure B,Shear Adhesion to a Standard(NIST)FiberboardAstrip of tape is applied to a panel covered withNIST SRM 1810A berboard under controlled roll down.The

19、panel is mounted vertically,a standard mass is attached to thefree end of the tape and the time to failure determined.3.3 Procedure C,Shear Adhesion to a Standard CENFiberboardAstrip of tape is applied to a panel covered withthe CEN standard berboard under controlled roll down.Thepanel is mounted ve

20、rtically,a standard mass is attached to thefree end of the tape and the time to failure is determined.3.4 Procedure D,Shear Adhesion to a Fiberboard withControlled Roll DownThe panel is mounted vertically,astandard mass is attached to the free end of the tape and thetime to failure is determined.3.5

21、 Procedure E,Shear Adhesion to a Standard SteelPanelA strip of lament reinforced tape is applied to astandard steel panel with a 120 bend at one end withcontrolled roll down.The panel is mounted horizontally,tapeside up,with the free end of the tape allowed to hang verticallyover the rounded end.A s

22、tandard mass is attached to the freeend of the tape and allowed to act for the specied time.3.6 Procedure F,Shear Adhesion of Filament ReinforcedTape to a Standard(NIST)FiberboardA strip of lamentreinforced tape is applied to a panel with a 120 bend,coveredwith NIST SRM 1810A standard berboard under

23、 controlledroll down.The panel is mounted horizontally,tape side up,withthefreeendofthetapeallowedtohangverticallyovertheround end of the panel.Astandard mass is attached to the freeend of the tape and allowed to act for a specied time.3.7 Procedure G,Shear Adhesion of a Filament ReinforcedTape to a

24、 CEN Standard FiberboardA strip of lamentreinforced tape is applied to a panel covered with CENstandard berboard under controlled roll down.The panel ismountedhorizontally,tapesideup,withthefreeendofthetapeallowed to hang vertically over the round end of the panel.Astandard mass is attached to the f

25、ree end of the tape andallowed to act for the specied time.3.8 ProcedureHThis procedure is conducted as describedin Procedure A except the test is conducted at an elevatedtemperature after a 10-min dwell time at the elevated tempera-ture.3.9 For Procedures A,B,C,D,and H the preferredspecimen size is

26、 12 by 12 mm 0.5 by 0.5 in.Aspecimen sizeof 24 by 24 mm 1 by 1 in.may be specied.3.10 For Procedures E,F and G the specimen width shall be12 mm 0.5 in.For testing reinforced lament by ProcedureH,the width shall be 12 mm 0.5 in.4.Signicance and Use4.1 ProcedureAmeasures the ability of a pressure-sens

27、itivetape to adhere to a standard steel panel under constant stress.This may or may not relate to the ability of the tape to adhereto other surfaces.4.2 Procedures B,C,and D may be used to determine theshear adhesion of the tapes generally used to close berboardboxes in packaging applications.4.3 Pr

28、ocedure D measures the shear adhesion of a pressure-sensitive tape to a nonstandard berboard,liner board,corru-gated board,or other surfaces which is agreed upon for testing.This may be used to compare the shear adhesion of a tape to aparticular berboard surface or to compare the shear adhesionof a

29、tape to a variety of berboard surfaces.4.3.1 The surfaces of similar berboards may exhibit con-siderable variation between mills,between batches from onemill,and within batches.Take care in the choice of samplesandwhencomparingresultsbetweenberboardsurfaceswhichmay not be exactly the same.4.3.2 The

30、precision of tests conducted on nonstandardsurfaces may be different than that described in Section 13.4.4 Procedures E,F,and G may be used to determine theability of a lament reinforced tape to hold when placed underconstant stress.4.5 ProcedureHmaybeusedtocomparetheshearadhesionof tape applied to

31、a standard steel surface and tested at anelevated temperature.The use of an elevated temperatureduring test tends to reduce the duration of the test.5.Apparatus5.1 Specimen Cutter5,6,7The specimen cutter shall holdtwo single-edge razor blades in parallel planes,a precisedistance apart,to form a cutt

32、er of exact specimen width.Two3AFERA(Association des Fabricants Europeen de Rubans Auto-Adhesifs),LAM,laan Copes van Cattenburch 79,NL2858 EW.,the Hague,the Netherlands.4EN(European Norm),available from COMITE Europeen de Normalisation,CEN Rue de Stassart,36,B-1050,Brussels,Belgium.5AvailablefromPST

33、C(PressureSensitiveTapeCouncil),400N.MichiganAve.,No.2200,Chicago,IL 606114267.6These widths correspond to the primary metric(SI)units described in GuideD5750/D5750M.These so-called“modular metric”units generally are usedthroughout the world.If it is desirable to test slightly different widths(for e

34、xample,25 of 50 mm)of specimens per 8.4,this should be noted per 12.1.6 and calculationsper 11.1 must account for the difference.7The sole source of supply of the apparatus known to the committee at this timeis Chemsultants International,9349 Hamilton Drive,Mentor,OH 440611118.Ifyou are aware of alt

35、ernative suppliers,please provide this information to ASTMInternational Headquarters.Your comments will receive careful consideration at ameeting of the responsible technical committee,1which you may attend.D3654/D3654M 06(2019)2 cutters,12 mm 0.5 in.and 24 mm 1 in.cutting width,shallbe available or

36、 appropriate alternates,which will not causeedge damage.NOTE 1The 12-mm 0.5-in.cutter shall consist of a 12-mm 0.5-in.thick by 200-mm 8-in.length of aluminum bar stock 12-mm 0.5-in.wide.The edges for about 125 mm 5 in.from one end shall be roundedslightly to form a handle.The width of the bar for 75

37、 mm 3 in.shall benarrowed to exactly 12 mm 0.5 in.minus the thickness of a singleedgerazor(one of two used as cutting edges).The razor shall be held inposition using side plates.The end of the cutter shall be cut away at a 45angle to expose the cutting edges at one end of the blades.The edges shallb

38、e separated by 12 6 0.10 mm 0.5 6 0.005 in.The 24 mm 1 in.cuttershall follow the same description except the bar stock shall be 24-mm1-in.wide and shall be narrowed to exactly 24 mm 1 in.minus thethickness of a single edge razor.5.2 Dispensing System,for solvents,such as a wash bottle.5.3 Panel5,7:5

39、.3.1 For ProceduresA,B,C,D,and H,a 50 by 125 mm 2by 5 in.not less than 1.1 mm 0.043 in.thickness 302 or 304stainless steel sheet with bright annealed nish in accordancewith Specication A666.The surface roughness height shall be50 6 25 nm 2.0 6 1.0 in.arithmetical average deviationfromameanline.Oneor

40、bothofthepanelendsshallbegroundto form a 90 angle with the panel surface.Panels showingstains,discolorations,or numerous scratches are not accept-able.New panels should be cleaned before use as described in10.1,exceptwithtenwashesofthenalsolvent.Betweenuses,the panels test surface shall be protected

41、 from scratches andcontamination,and the panels stored at conditions described in8.1.5.3.2 For Procedures E,F,and G,a panel as described in5.3.1shallhavea12mm0.5in.lengthatoneendofthepanelbent through an arc of 120 away from the test surface.Theradius of the curvature of the nished surface at the be

42、nd shallbe 1.5 to 3 mm 116 to18 in.5.4 Roller,mechanically or hand-operated.5,75.4.1 Asteelroller85 62.5mm3.25 60.1in.indiameterand 45 6 1.5 mm 1.75 by 0.5 in.in width,covered withrubber approximately 6 mm 0.25 in.in thickness,having aShore scaleAdurometer hardness of 80 6 5.The surface shallbe a tr

43、ue cylinder void of any convex or concave deviations.The mass of the roller shall be 2040 6 45 g 4.5 6 0.1 lb.5.4.2 No part of the apparatus shall increase the mass of theroller during use.The roller shall move either mechanically orby hand at the rate of 10 6 0.4 mm/s 24 6 0.5 in./min.5.5 Test Stan

44、ds and Ancillary Apparatus:5,75.5.1 Procedures A,B,C,D,and HA test stand that shallholdthetestpanel,withtapeapplied,atanangleof0to2withthe vertical,so that when the mass is acting on the testspecimen,no peel forces will be exerted on the tape.5.5.2 ProceduresE,G,andFAtest stand that will supportthe

45、test panel in a horizontal plane,approximately 300 mm 12in.above the work surface.5.5.3 ClamporHook,thatwillallowattachmentofthemassto the specimen,distributing the load equally across the tapespecimen width.5.5.4 Test Masses:5.5.4.1 Procedures A,B,C,D,and HThe test mass shallbe 1000 6 5 g or other

46、mass as specied.The mass of theclamp or hook described in 5.5.3 shall be included as part ofthe total mass.5.5.4.2 Procedures E,F,and GThe test mass shall be 4.56 0.2 kg 10 6 0.5 lb or other mass as specied.The mass ofthe clamp or hook as described in 5.5.3 shall be included in thetotal mass.5.5.5 T

47、iming Systems:5.5.5.1 ProcedureA,B,C,D,and H to measure the intervalin minutes,between the application of the load to the specimenand its separation from the panel.5.5.5.2 Procedures E,F,and G,a suitable means of mea-suring the amount of slippage of the tape to 1 mm 164 in.onthe panel after the mass

48、 has acted for 48 h.6.Reagent Materials6.1 Purity of ReagentsReagent grade chemicals shall beused in all tests.Other grades may be used,provided it is rstascertained the reagent is of sufficiently high purity to permitits use without lessening the accuracy of the determination.6.2 Solvents:6.2.1 Any

49、 of the following solvents may be used forcleaning.NOTE 2Before selecting or using these solvents for cleaning testpanels be sure to read and follow all precautions on the chemical MaterialSafety Data Sheets(MSDS)and consult with Environmental,Health andSafety(EHS)Professionals.6.2.1.1 Diacetone alc

50、ohol nonresidual,technical grade orbetter.6.2.1.2 Methanol(95%).6.2.1.3 Methyl Ethyl Ketone(MEK).6.2.1.4 n-Heptane.6.2.1.5 Acetone.6.2.2 For referee testing,the nal cleaning shall be withMEK or acetone.6.3 Cleaning Material,absorbent,surgical gauze,cottonwool,or tissue.To be suitable,materials must